Document Type

Article

Original Publication Date

2009

Journal/Book/Conference Title

Journal of Applied Physics

Volume

105

Issue

11

DOI of Original Publication

10.1063/1.3132799

Comments

Originally published at http://dx.doi.org/10.1063/1.3132799

Date of Submission

November 2015

Abstract

We have used conducting atomic force microscopy (CAFM) to study the morphology and electronic behavior of as-received and air-annealed (0001) Zn- and (0001¯) O-polar surfaces of bulk ZnO. Both polar surfaces exhibit relatively flat morphologies prior to annealing, which rearrange to form well-defined steps upon annealing in air at 1050 °C for 1 h. Long-term exposure to air results in surface layer pitting and the destruction of steps for both the as-received and air-annealed (0001¯)surfaces, indicating its enhanced reactivity relative to the (0001) surface. CAFM I-V spectra for polar surfaces are similar and indicate Ohmic to rectifying behavior that depends on the maximum applied ramp voltage, where higher voltages result in more conducting behavior. These data and force-displacement curves suggest the presence of a physisorbed H2O layer, which is removed at higher voltages and results in higher conduction.

Rights

Moore, J. C., Kenny, S. M., & Baird, C. S., et al. Electronic behavior of the Zn- and O-polar ZnO surfaces studied using conductive atomic force microscopy. Journal of Applied Physics, 105, 116102 (2009). Copyright © 2009 American Institute of Physics.

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